|
KMID : 1023520220450030237
|
|
Korean Journal of Veterinary Service
2022 Volume.45 No. 3 p.237 ~ p.242
|
|
|
Validation of simultaneous mycotoxin analysis method in pet food using LC-MS/MS
|
|
Choi Yoon-Hwa
Ahn Woo-Seok
Kim Ji-Eun
Kim Doo-Hwan
|
|
|
Abstract
|
|
|
|
The simultaneous analysis of mycotoxins using LC-MS/MS, a food official analysis method, was applied with compound feed for pets with high consumer preferences. In this study, the linearity of all calibration curves showed good linearity of 0.99 or more. and both the accuracy (recovery rate) and precision (repeatability) criteria of the concentration range for each mycotoxin in the National Agricultural Products Quality Management Service's Validation and Verification Guidelines were met. And as a result of analyzing FAPAS QCM in the same way, it was assesed that the z-scores of Aflatoxin B1, Ochratoxin A, Zearalenone, and Fumonisin B1, were within ±2 range. This study showed that the application of the food official analysis method to compound feed for pets is suitable.
|
|
|
KEYWORD
|
|
|
Validation of mycotoxin, Pet food, LC-MS/MS
|
|
|
FullTexts / Linksout information
|
|
|
|
|
|
Listed journal information
|
|
|
|