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KMID : 0615219860110010095
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Journal of Kwangju Health
1986 Volume.11 No. 1 p.95 ~ p.101
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A Study on the Synthesis of Mo(Ⅴ) and Mo(Ⅳ) Complexes by the Electro-Reduction Method
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이송주/Lee SJ
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Abstract
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(NH₄)₂Mo(V)OCl_(5) and(PyH)₂ Mo(Ⅳ)(SCN)_(6) complexes, molybdenum(Ⅴ)and (Ⅳ) oxidated state are syntlietized by the electro-reduction method, which has been operated easily in using the following electric cell; C ｜ Cone HCl∥MoO₃-SN-HCl｜ Hg at applied, voltage hold constant 3 volt and the current from 1.5∼2.0 amp. with a galv-anometer, these properties and composition of complexes have been identified with an elental analysis, IR-Spectra and T. G. A.
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KEYWORD
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